The crystal and molecular structure of 2,7-diazanaphthalene

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Huiszoon, C. and Hummel, G.J. van and Ham, D.M.W. van den (1977) The crystal and molecular structure of 2,7-diazanaphthalene. Acta Crystallographica Section B: Structural crystallography and crystal chemistry, 33 . pp. 1867-1870. ISSN 0567-7408

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Abstract:X-ray diffraction data were collected at 20°C on a computer-controlled Philips diffractometer (PW 1100). The structure was solved by direct methods and refined by the full-matrix least-squares method to an R of 0.065 (weighted R 0.046). The molecule in the crystal is of lower symmetry than C2,.. The geometry of the molecule has been compared with NMR results obtained by Danieli, Lunazzi & Veracini [J. Chem. Soc. Perkin II, (1976), pp. 19-201. As a result a C-H bond-length correction of 0.09 (2) A was found.
Item Type:Article
Copyright:© 1977 International Union of Crystallography
Link to this item:http://purl.utwente.nl/publications/59235
Official URL:http://dx.doi.org/10.1107/S0567740877007225
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