Synthesis of neutral, water-soluble calix[4]arenes

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Grote Gansey, Marcel H.B. and Steemers, Frank J. and Verboom, Willem and Reinhoudt, David N. (1997) Synthesis of neutral, water-soluble calix[4]arenes. Synthesis, 1997 (6). pp. 643-648. ISSN 0039-7881

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Abstract:Novel neutral water-soluble calix[4]arenes were synthesized via chlorosulfonylation of lower rim functionalized calix[4]arenes followed by reaction with hydroxyl group containing amines. The solubility of these calix[4]arenes sulfonamides in water varies from ∼ 10-5 to 3.1⋅10-1 M. A route via hydrophobically protected amines improves the purification.
Item Type:Article
Copyright:© Georg Thieme Verlag 1997
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Science and Technology (TNW)
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Link to this item:http://purl.utwente.nl/publications/11125
Official URL:http://dx.doi.org/10.1055/s-1997-4506
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Metis ID: 106006