The effect of phase inversion during semibatch aromatic nitrations

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Zaldivar, J.M. and Alos, M.A. and Molga, E.J. and Hernandez, H. and Westerterp, K.R. (1995) The effect of phase inversion during semibatch aromatic nitrations. Chemical Engineering and Processing, 34 (6). pp. 529-542. ISSN 0255-2701

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Abstract:The effect of phase inversion during semibatch aromatic nitrations is experimentally characterized and analysed. The influence of various parameters, i.e. interfacial area, effective heat-transfer coefficient and overall mass-transfer coefficient, is studied. The implications for optimizing nitrations are discussed from performance and safety points of view. The accumulation of unreacted nitric acid can be dangerous if accompanied by a phase inversion, owing to the fact that the rate may increase suddenly.
Item Type:Article
Copyright:© 1995 Elsevier Science
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Link to this item:http://purl.utwente.nl/publications/10868
Official URL:http://dx.doi.org/10.1016/0255-2701(95)04110-9
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Metis ID: 105878